This is fundamentally impossible.
In the metric for the black hole, $G$ only ever appears in the combination $GM$. Consequently, there is no way of interacting with a black hole that will allow you to independently measure the mass $M$ and $G$.
The same is true for the dynamics of a black hole binary. G will always be paired with one of the masses (and vice versa).
Not coincidentalycoincidentally, the same is true in Newtonian gravitational physics, which is why we don't know $GM_{\odot}$ very accurately, but not G.