I'm having a hard time finding data about an experiment that I know has been done a bunch of times:
I have a sheet of rutile TiO2 (110) that I want to reduce to various TiO(2-x) forms where the x is what I want to vary. To do this reduction, I have a high temp oven that I can fill with H2 or simply fill with a vacuum. I need a chart that will tell me what temp, partial pressure of H2, and duration I need to convert my sheets surface to a desired reduced value (i.e. I want a specific x).
I then want to reoxidize the surface by using lower temperatures in a furnace that I can fill with oxygen at different pressures. I need a chart that will tell me what temp, partial pressure of O2, and duration I need to re-Oxidize the surface.
The goal here is not to simply get the surface, but to test other properties. I was hoping this step (finding the proper charts) would have been fairly straightforward, but my literature searches haven't turned up quite what I need. I was hoping someone here can point me to a resource that has this data so I can get on with my getalong.